刊名 |
Medicinal Plant |
作者 |
Zhenying FU, Bing QING, Yinghong HUANG, Xianyi SHI, Meiyan QIU, Xian PENG, Jiangcun WEI, Fengzhen LI, Wen ZHONG |
作者单位 |
Guangxi International Zhuang Medical Hospital |
DOI |
10.19601/j.cnki.issn2152-3924.2024.01.018 |
年份 |
2024 |
刊期 |
1 |
页码 |
71-74 |
关键词 |
Jiedu Shengxue granules, Thin layer identification, Notoginsenoside R1, Quality standard |
摘要 |
[Objectives] To establish the quality standard of hospital preparation Jiedu Shengxue granules. [Methods] Scleromitrion diffusum and Prunella vulgaris in Jiedu Shengxue granules were qualitatively identified by thin layer chromatography (TLC). A high performance liquid chromatography (HPLC) was established to determine the content of notoginsenoside R1 in the granule. [Results] The traditional Chinese medicinal materials in Jiedu Shengxue granules could be identified by TLC, and the characteristic spots were stable and clear. Notoginsenoside R1 had a good linear relationship in the range of 10.45-104.5 μg/mL, with an average recovery of 98.52% and RSD=2.36%. [Conclusions] TLC and HPLC, as the quality control methods of Jiedu Shengxue granules, have high accuracy and good repeatability, which lays a foundation for the quality control of this mixture. |